|
| C.没有。 |
13C核磁共振(101 (兆赫)δ |
1.核磁共振氢谱(400 (兆赫)δ |
|
| 2. |
156.34 |
— |
| 3. |
133.27 |
— |
| 4. |
177.53 |
— |
| 5. |
156.49 |
— |
| 6. |
98.84 |
6.20(d,J = 2.1 赫兹,1H) |
| 7. |
164.59 |
— |
| 8. |
93.79 |
6.43(d),J = 2 赫兹,1H) |
| 9 |
161.29 |
— |
| 10 |
104.01 |
— |
| 1′ |
120.99 |
— |
| 2′ |
130.97 |
8.05(d,J = 8 赫兹,2小时) |
| 3′ |
115.20 |
6.87(t,J = 8 赫兹,2小时) |
| 4′ |
160.03 |
— |
| 5′ |
115.20 |
6.87(t,J = 8 赫兹,2小时) |
| 6′ |
130.97 |
8.05(d,J = 8 赫兹,2小时) |
| 1″ |
100.98 |
5.45(d),J = 7.5 赫兹,1H) |
| 2″ |
74.30 |
3.18 |
| 3″ |
77.54 |
3.09(d),J = 5 赫兹,2小时) |
| 4″ |
69.98 |
3.09(d),J = 5 赫兹,2小时) |
| 5″ |
76.50 |
3.21 |
| 6″ |
60.93 |
3.56, 3.32 |
|
|