分析方法在化学杂志》上/2011年/文章/选项卡3

研究文章

测定钾、钠和总碱在波特兰水泥、粉煤灰、外加剂和水混凝土的一个简单的流动注射火焰光度系统

表3

内容的钠、钾、总碱由FI-FES和分批菲斯的方法。

样本 % Na2O % K2O %总碱
FI-FES 菲斯 FI-FES 菲斯 FI-FES 菲斯

水泥
1 0 1 2 4 ± 0 0 0 1 0 1 2 1 ± 0 0 0 1 0 2 9 9 ± 0 0 0 2 0 2 9 2 ± 0 0 0 1 0.321 0.313
2 0 2 6 7 ± 0 0 0 2 0 2 6 2 ± 0 0 0 1 0 3 3 2 ± 0 0 0 4 0 3 2 2 ± 0 0 0 2 0.485 0.474
3 0 1 2 2 ± 0 0 0 1 0 1 1 7 ± 0 0 0 1 0 2 6 8 ± 0 0 0 2 0 2 6 5 ± 0 0 0 1 0.299 0.291
4 0 0 5 2 ± 0 0 0 1 0 0 4 7 ± 0 0 0 1 0 0 5 3 ± 0 0 0 1 0 0 4 5 ± 0 0 0 1 0.087 0.076
5 0 4 3 7 ± 0 0 0 2 0 4 3 5 ± 0 0 0 2 0 6 0 0 ± 0 0 0 7 0 6 3 7 ± 0 0 0 3 0.831 0.855
6 0 0 7 6 ± 0 0 0 1 0 0 7 0 ± 0 0 0 1 0 1 3 1 ± 0 0 0 2 0 1 2 8 ± 0 0 0 1 0.162 0.155
7 0 1 0 8 ± 0 0 0 1 0 1 0 7 ± 0 0 0 1 0 2 7 7 ± 0 0 0 2 0 2 7 3 ± 0 0 0 1 0.291 0.286
8 0 1 3 9 ± 0 0 0 1 0 1 3 4 ± 0 0 0 1 0 2 9 4 ± 0 0 0 4 0 2 9 0 ± 0 0 0 1 0.333 0.325
9 0 0 9 8 ± 0 0 0 2 0 0 9 1 ± 0 0 0 1 0 2 4 9 ± 0 0 0 3 0 2 4 7 ± 0 0 0 1 0.262 0.254
10 0 1 1 8 ± 0 0 0 1 0 1 1 3 ± 0 0 0 1 0 3 2 6 ± 0 0 0 5 0 3 2 6 ± 0 0 0 1 0.333 0.327
粉煤灰
11 0 0 7 9 ± 0 0 0 2 0 0 7 4 ± 0 0 0 1 0 0 3 9 ± 0 0 0 1 0 0 3 5 ± 0 0 0 1 0.104 0.098
12 0 0 2 6 ± 0 0 0 1 0 0 2 3 ± 0 0 0 1 0 0 3 5 ± 0 0 0 1 0 0 3 3 ± 0 0 0 1 0.049 0.045
13 1 6 0 8 ± 0 0 3 5 1 5 9 5 ± 0 0 0 8 1 3 3 9 ± 0 0 1 6 1 4 5 5 ± 0 0 0 7 2.489 2.553
14 0 5 4 7 ± 0 0 0 6 0 5 7 4 ± 0 0 1 3 0 5 7 1 ± 0 0 1 3 0 6 2 7 ± 0 0 0 1 0.922 0.986
15 0 1 5 5 ± 0 0 0 4 0 1 4 7 ± 0 0 0 1 0 1 7 2 ± 0 0 0 2 0 1 6 7 ± 0 0 0 1 0.268 0.257
16 1 6 6 4 ± 0 0 3 7 1 6 5 8 ± 0 0 0 8 1 4 0 7 ± 0 0 1 2 1 5 5 2 ± 0 0 0 7 2.590 2.680
17 1 9 8 9 ± 0 0 1 6 1 9 8 3 ± 0 0 0 8 1 5 4 3 ± 0 0 1 7 1 6 6 4 ± 0 0 0 7 3.005 3.077
18 0 0 9 8 ± 0 0 0 1 0 0 9 3 ± 0 0 0 1 0 1 7 7 ± 0 0 0 3 0 1 7 4 ± 0 0 0 1 0.214 0.207
19 1 7 7 1 ± 0 0 3 4 1 7 6 3 ± 0 0 0 8 1 4 9 0 ± 0 0 0 5 1 6 3 9 ± 0 0 0 7 2.751 2.841
20 1 8 3 9 ± 0 0 2 3 1 8 3 7 ± 0 0 1 5 1 3 3 3 ± 0 0 0 6 1 4 6 1 ± 0 0 1 2 2.715 2.798
掺合料
21 0 1 5 9 ± 0 0 0 1 0 1 6 2 ± 0 0 0 1 0 0 1 4 ± 0 0 0 1 0 0 1 2 ± 0 0 0 1 0.168 0.171
22 0 1 5 8 ± 0 0 0 3 0 1 5 9 ± 0 0 0 1 0 0 0 8 ± 0 0 0 1 0 0 0 5 ± 0 0 0 1 0.164 0.162
23 0 1 5 3 ± 0 0 0 5 0 1 5 0 ± 0 0 0 3 0 0 2 0 ± 0 0 0 1 0 0 1 7 ± 0 0 0 1 0.166 0.161
24 4 5 8 4 ± 0 0 9 9 4 5 5 5 ± 0 0 1 4 0 0 1 4 ± 0 0 0 1 0 0 1 1 ± 0 0 0 1 4.593 4.562
25 2 1 8 2 ± 0 0 2 6 2 1 6 5 ± 0 0 0 8 0 1 8 6 ± 0 0 0 1 0 1 9 9 ± 0 0 0 1 2.305 2.296
26 0 1 5 7 ± 0 0 0 5 0 1 5 3 ± 0 0 0 3 0 0 1 7 ± 0 0 0 1 0 0 1 5 ± 0 0 0 1 0.168 0.163
27 0 1 9 5 ± 0 0 0 1 0 1 8 6 ± 0 0 0 1 0 0 1 6 ± 0 0 0 1 0 0 1 3 ± 0 0 0 1 0.206 0.195
28 0 1 6 1 ± 0 0 0 1 0 1 5 7 ± 0 0 0 1 0 0 1 2 ± 0 0 0 1 0 0 1 0 ± 0 0 0 1 0.169 0.164
29日 0 1 7 0 ± 0 0 0 6 0 1 6 7 ± 0 0 0 1 0 0 0 9 ± 0 0 0 1 0 0 0 5 ± 0 0 0 1 0.175 0.170
30 0 1 7 8 ± 0 0 0 5 0 1 6 8 ± 0 0 0 1 0 0 2 2 ± 0 0 0 1 0 0 2 2 ± 0 0 0 1 0.192 0.183
31日 0 2 0 3 ± 0 0 0 4 0 1 9 7 ± 0 0 0 1 0 0 4 3 ± 0 0 0 1 0 0 4 3 ± 0 0 0 1 0.232 0.225
32 0 1 9 6 ± 0 0 0 4 0 1 9 4 ± 0 0 0 1 0 0 4 3 ± 0 0 0 1 0 0 4 3 ± 0 0 0 1 0.224 0.223
33 0 1 9 0 ± 0 0 0 1 0 1 8 6 ± 0 0 0 1 0 0 4 4 ± 0 0 0 1 0 0 4 5 ± 0 0 0 1 0.219 0.216
34 0 2 3 5 ± 0 0 0 5 0 2 3 4 ± 0 0 0 1 0 0 4 8 ± 0 0 0 1 0 0 5 0 ± 0 0 0 1 0.267 0.267
35 0 2 3 9 ± 0 0 0 5 0 2 2 7 ± 0 0 0 1 0 0 5 1 ± 0 0 0 2 0 0 5 3 ± 0 0 0 1 0.272 0.261

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