研究文章
同时定量测定多酚类化合物艾纳香属balsamifera的高效液相色谱(Ai-Na-Xiang Sembung)与光电二极管阵列检测器
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| 不。 |
复合名称 |
校准曲线一个 |
R2 |
线性范围(μg / mL) |
LODb(μg / mL) |
定量限c(μg / mL) |
|
| 1 |
芦丁 |
y= 36771x+ 4732.7 |
0.9997 |
0.37∼139.92 |
0.18 |
0.37 |
| 2 |
Hyperoside |
y= 45866x−25252 |
0.9999 |
0.34∼126.65 |
0.10 |
0.34 |
| 3 |
异槲皮苷 |
y= 45714x−5732.6 |
0.9999 |
0.31∼117.20 |
0.10 |
0.31 |
| 4 |
3、3′,5、7-Tetrahydroxy-4′-methoxyflavanone |
y= 6982.1x−19647 |
0.9999 |
2.67∼1001.40 |
0.89 |
2.67 |
| 5 |
3′,5′,7-Tetrahydroxyflavanone |
y= 7495.0x−9796.1 |
1.0000 |
6.61∼330.47 |
1.32 |
5.29 |
| 6 |
槲皮素 |
y= 50230x−22534 |
0.9999 |
1.15∼57.34 |
0.23 |
0.92 |
| 7 |
3、3′,4′,5-Tetrahydroxy-7-methoxyflavanone |
y= 5499.5x−15331 |
0.9997 |
3.55∼443.52 |
0.88 |
3.55 |
| 8 |
Chrysosplenol C |
y= 39377x−14116 |
0.9998 |
0.21∼51.55 |
0.07 |
0.21 |
| 9 |
Diosmetin |
y= 1.0E+ 5x−14906 |
1.0000 |
0.10∼36.06 |
0.03 |
0.10 |
| 10 |
Tamarixetin |
y= 64551x−12598 |
0.9997 |
0.11∼28.06 |
0.04 |
0.11 |
| 11 |
3、5、7-Trihydroxy-3′, 4′-dimethoxyflavone |
y= 70721x−19615 |
0.9999 |
0.11∼95.68 |
0.04 |
0.11 |
| 12 |
3、3′,5-Trihydroxy-4′, 7-dimethoxyflavanone |
y= 7271.0x−5822.3 |
1.0000 |
0.86∼747.94 |
0.29 |
0.86 |
| 13 |
Blumeatin |
y= 7339.9x−8361.5 |
1.0000 |
0.72∼627.09 |
0.24 |
0.72 |
| 14 |
鼠李亭 |
y= 46787x−11774 |
1.0000 |
0.20∼175.73 |
0.07 |
0.20 |
| 15 |
3′,4′,5-Trihydroxy-3 7-dimethoxyflavone |
y= 88162x−11165 |
0.9996 |
0.06∼22.04 |
0.02 |
0.06 |
| 16 |
Xanthoxylin |
y= 10671x−5373.4 |
1.0000 |
0.99∼173.27 |
0.33 |
0.99 |
| 17 |
Ombuin |
y= 1.9E+ 5x−18006 |
0.9999 |
0.07∼23.66 |
0.02 |
0.05 |
| 18 |
3,5-Dihydroxy-3′, 4′, 7-trimethoxyflavone |
y= 74640x−9102.7 |
0.9999 |
0.08∼20.18 |
0.03 |
0.08 |
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y峰面积和吗x化合物的浓度(μg / mL)。bLOD指的检测极限,S / N = 2.3 - -3.6: 1。c定量限是指量化的限制,S / N = 8.1 - -10.3: 1。
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